In this study, microstructural and crystallographic properties of phase transformations occurring with thermal effect in Fe-XMn-Mo-Si (X = 15.14wt.% ve 18.45wt.%) alloys have been investigated. The effects of (wt.%) Mn rates in the alloy on the characteristics of phase transformations were investigated by using Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM) and X-Ray Diffraction (XRD). SEM and TEM investigations was observed that two different martensite (ε and α') structures were formed in austenite grain. In addition, in TEM observations, the interface regions were selected over the bright field image. Crystallographic orientation relationships were obtained by the analyses of electron diffraction patterns from the interface regions. γ → α' type transformation was observed for α' particle formation, and orientation relationship was found as (1–11)γ // (011)α', [101]γ // [1–11–]α' and, γ → ε type transformation was observed for ε martensite plate formation, and the orientation relationship was found as (1–11–)γ // (0002–)ε, [1–1–0]γ // [2–110]ε. It was noticed that this orientation relationships were compatible with the literature (Kurdjumov-Sachs and Shoji-Nishiyama orientation relationship). Precipitation phase (carbide) formation was observed in microstructure analyses. The changes in the magnetic properties of the alloys having different rates of Mn as a consequence of thermal effect phase transformations was investigated by using Mössbauer Spectroscopy. The internal magnetic field, volume fractions (transformation rates), isomer shift values and magnetic characteristics of the main and product phases were revealed by Mössbauer Spectroscopy. In the Mössbauer Spectrum, it was noticed that ε-martensite and γ-austenite structures showed paramagnetic single-peak, and α'-martensite showed ferromagnetic six-peaks.
The results of the detailed seismoacoustic profilling (CSP, boomar) are presented. The investigation has been carried out in February 1985 and 1988 during two Geodynamical Expeditions organized by the Institute of Geophysics of the Polish Academy of Sciences. The boomar penetration of the caldera floor went down to 150 msec. Four seismoacoustic units of volcanic formations have been determined. The unit A corresponds to pre-caldera series and occurred only in the border part of the flooded caldera. The unit contains mainly pyroclastic rocks (consolidated agglomerates and tuffs) and probably some intercalations of lavas. The units B, C and D fill up the caldera bottom and correspond to post-caldera series. The units are composed of pyroclastic rocks, containing also materials redeposited by lahars, glaciers, landwaters and by wind. The units C and D (the youngest one) were certainly deposited under water. All the units are cut by numerous faults, vents and other types of intrusions. The larger faults, en echelon type, are situated around the bottom and form a ring-fracture. Caldera was formed by succesive stages of collapsing. This process is not finished yet and volcanic activity is still alive (especially in the western part of the flooded caldera).
The data aggregation process of wireless sensor networks faces serious security problems. In order to defend the internal attacks launched by captured nodes and ensure the reliability of data aggregation, a secure data aggregation mechanism based on constrained supervision is proposed for wireless sensor network, which uses the advanced LEACH clustering method to select cluster heads. Then the cluster heads supervise the behaviors of cluster members and evaluate the trust values of nodes according to the communication behavior, data quality and residual energy. Then the node with the highest trust value is selected as the supervisor node to audit the cluster head and reject nodes with low trust values. Results show that the proposed mechanism can effectively identify the unreliable nodes, guarantee the system security and prolong the network lifetime.