In this study, the electrospray deposition (ESD) method was used to deposit carbon nanotubes (CNT) onto the surfaces of carbon fibers (CF) in order to produce hybrid carbon fiber-carbon nanotubes (CF-CNT) which is rarely reported in the past. Extreme high-resolution field emission scanning electron microscopy (XHR-FESEM), high-resolution transmission electron microscopy (HRTEM) and x-ray photoelectron spectroscopy (XPS) were used to analyse the hybrid carbon fiber-carbon nanotube (CF-CNT). The results demonstrated that CNT was successfully and homogenously distributed on the CF surface. Hybrid CF-CNT was then prepared and compared with CF without CNT deposition in terms of their tensile properties. Statistically, the tensile strength and the tensile modulus of the hybrid CF-CNT were increased by up to 3% and 25%, respectively, as compared to the CF without CNT deposition. The results indicated that the ESD method did not cause any reduction of tensile properties of hybrid CF-CNT. Based on this finding, it can be prominently identified some new and significant information of interest to researchers and industrialists working on CF based products.

The Reinforced Concrete (RC) beams containing Expanded Polystyrene Beads (EPS) and Palm Oil Fuel Ash (POFA) as sand and cement replacement with a percentage between 10% and 30% were studied in terms of load-deflection behaviour. RC beam’s size was 1000×150×150 mm and simply supported at spaced 750 mm apart. The 10% of POFA without EPS shows a slight increase which is 0.26% higher than normal concrete in compressive strength. The ultimate load and flexural performance of RC beams with EPS and POFA exhibited a decreasing trend. All beams’ ultimate load exceeds the design value. The cracks of the RC beam may be classified as vertical flexural cracks, and some of the cracks can be classified as shear cracks based on the crack angle. As the percentage of EPS and POFA increases above 20% for all specimens, cracking starts to change to shear cracking.