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Abstract

The aim of the hereby paper is to present the developed model of determining the volume and surface porosity based on the main fraction

of polifractional materials, its experimental verification and utilisation for the interpretation of effects accompanying the formation of a

moulding sand apparent density, porosity and permeability in the blowing processes of the core and moulds technology.

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Authors and Affiliations

R. Dańko
J. Dańko
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Abstract

Foundry sand is the main element of sand mixtures from which molds or sand cores are made. Due to the continuous development of coremaking technologies, the selection of the right type of base sand becomes more and more important. The major features of foundry sand are determined by the following factors: chemical and mineralogical composition, sand grain size, grain size distribution, sand grain shape, and surface quality. The main goal of our research was to develop a qualification method that can be used to predict the characteristics of sand cores made from different sand types. Samples made from different types of foundry sand were used during the research whose properties were examined with a new qualification system, and then its connection with the gas permeability of sand cores was analyzed. Based on the research results, a strong correlation could be established between the suggested quality indicators: CQi (Core Quality Index), CG (Coefficient of Granulometry), and permeability.
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Bibliography

[1] Stauder, B.J. (2018). Investigation on the removal of internal sand cores from aluminium castings. Dissertation, Montanuniversitäte, University of Leoben, Leoben, Austria.
[2] Schindelbacher, G. & Kerber H. (2013). Umfassende Charakterisierung von Formstoffen mit einer neuen Prüfmethode. Giesserei Rundschau. 60 Heft 3/4, 58-66.
[3] Geraseva, O. (2016). P otential alternativer Formstoffe zur Kernherstellung. Masterarbeit, Montanuniversitäte, University of Leoben, Leoben, Austria.
[4] Conev, M., Vasková, I., Hrubovčáková, M. & Hajdúch, P. (2016). Impact of Silica Sand Granulometry on Bending Strength of Cores Produced by ASK Inotec Process. Manufacturing Technology. 16(2), 327-334. DOI: 10.21062/ujep/x.2016/a/1213-2489/MT/16/2/327.
[5] Vasková, I., Varga, L., Prass, I., Dargai, V., Coney, M., Hrubovčáková, M., Bartošová, M., Buľko, B. & Demeter P. (2020). Examination of Behavior from Selected Foundry Sands with Alkali Silicate-Based Inorganic Binders. Metals. 10(2), 235. DOI: 10.3390/met10020235.
[6] Flemming, E., Tilch, W. (1993). Formstoffe und Formverfahren. Deutscher Verlag fur Grundstoffindustrie, Leipzig – Stuttgart.
[7] Dańko, R. (2017). Influence of the Matrix Grain Size on the Apparent Density and Bending Strength of Sand Cores. Archives of Foundry Engineering. 17(1), 27-30. DOI: 10.1515/afe-2017-0005.
[8] Beňo, J. & Adamusová K. & Merta V. & Bajer T. (2019) Influence of Silica Sand on Surface Casting Quality. Archives of Foundry Engineering. 19(2), 5-8. DOI: 10.24425/afe.2019.127107.
[9] Marinšek, M., Zupan, K. (2011). Influence of the granulation and grain shape of quartz sands on the quality of foundry cores, Materials and Technology. 45 (5), 451-455.
[10] Löchte, K. (1998.) Working with the Cold Box Process in the Coremaking Department of a Foundry. Retrieved January 29, 2021, from: http://metkoha.com/documents/Working% 20with%20the%20Coldbox%20Process1.pdf.
[11] Bechný, V. (2012). Zukünftige Herausforderungen an Gießereisande. Giesserei-Rundschau. 59. Heft 3/4, 81-83.
[12] Kotzmann, J. & Bechný V. (2013). Die Zukunft der Form- und Kernherstellung. Retrieved January 29, 2021, from: http://www.giba.at/pdf/giba-de.pdf.
[13] Iden, F., Pohlmann, U., Tilch, W. & Wojtas, H.J. (2011). Strukturen von Cold-Box-Bindersystemen und die Möglichkeitihrer Veränderung. Giesserei Rundschau. 58, 1/2, 3-8.
[14] Iden, F., Tilch, W. & Wojtas, H.J. (2011). Die Haftungsmechanismen von Cold-Box-Bindemitteln auf der Formstoffoberfläche. Giesserei. 5/2011, 24-36.
[15] Dargai, V., Polzin, H., Varga, L., Dúl, J. (2015). Determination of granulometric properties of foundry sands with image analysis. (Öntödei homokok granulometriai tulajdonságainak meghatározása képelemzéssel). MultiScience - XXIX. microCAD International Multidisciplinary Scientific Conference, 9-10 April 2015. University of Miskolc – Miskolc, Hungary.
[16] Dargai, V., Polzin, H. & Varga, L. (2018). Die Bestimmung der granulometrischen Eigenschaften von Gießereisanden mittels dynamischer Bildanalyse. Giesserei Praxis. 4/2018, 19-22.
[17] Bodycomb, J. (2018). Size and shape of Particles from Dynamic Image Analysis. Retrieved January 29, 2021, from: https://www.slideshare.net/HORIBA/size-and-shape-of-particles-from-dynamic-image-analysis.
[18] Microtrac MRB (2017). Comparison Between Dynamic Image Analysis, Laser Diffraction and Sieve Analysis. Retrieved January 29, 2021, from: https://www.azom.com/article.aspx?ArticleID=14331.
[19] Raatz, G. (2014). Trends in der Partikelgrößenanalyse. Powtech / Technopharm – Messtechnik. 9/2014, 25-28. [20] Ridsdale and Ridsdale DieterT. Foundry sand testing equipment operating instructions (AFS). Catalogue No. 800, Retrieved January 29, 2021, from: https://www.basrid.co.uk/ridsdale/images/pdf/AFS_OIM.pdf

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Authors and Affiliations

H. Hudák
1
G. Gyarmati
1
L. Varga
1

  1. Institute of Foundry, Faculty of Materials Science and Engineering, University of Miskolc, Hungary
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Abstract

We used cytological and embryological methods to study reproductive cycle stages in Cerasus fruticosa Pall., Cerasus × eminens (Beck) Buia and Cerasus × mohacsyana (Kárpáti) Janchen from SW Slovakia, focusing on development of the male and female reproductive organs, fertilization processes and embryo formation. We found that reproductive potential was reduced by synergistic effects of negative biotic and abiotic factors. Despite the presence of degenerated, deformed pollen grains and their great variability of shape and size, a sufficient amount of normally developed viable pollen grains developed in anthers of C. fruticosa and C. × mohacsyana. Disturbed microsporogenesis in C. × eminens led to significantly lower production of viable pollen grains. We did not observe serious disturbances during megasporogenesis and megagametogenesis. Lower fruit set was caused by degeneration of ovules as a result of unsuccessful pollination, fertilization failure, or embryo degeneration during its initial development.

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Authors and Affiliations

Renáta Chudíková
Ľuba Ďurišová
Tibor Baranec
Pavol Eliáš
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Abstract

Later harvest time increased the infection of stems by Fusarium spp. and plant lodging. With the delay of harvest, the dry matter content in grain increased, but the crop in the later periods decreased. The optimal harvest time seems to be 20 days after reaching physiological maturity. In spite of using different genotypes and a wide range of harvest dates, the chemical analysis used to determine the presence of trichothecens B (DON, 3-AcDON, 15-AcDON and NIV) did not reveal their presence above the detection limit 0,001 mg/kg.
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Authors and Affiliations

Tadeusz Michalski
Juliusz Perkowski
Jerzy Stachowiak
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Abstract

Studies were conducted on a zinc coating produced on the surface of ductile iron grade EN-GJS-500-7 to determine the eutectic grain

effect. For this purpose, castings with a wall thickness of 5 to 30 mm were made and the resulting structure was examined. To obtain a

homogeneous metal matrix, samples were subjected to a ferritising annealing treatment. To enlarge the reaction surface, the top layer was

removed from casting by machining. Then hot dip galvanising treatment was performed at 450°C to capture the kinetics of growth of the

zinc coating (in the period from 60 to 600 seconds). Analysing the test results it was found that within the same time of hot dip

galvanising, the differences in the resulting zinc coating thickness on samples taken from castings with different wall cross-sections were

small but could, particularly for shorter times of treatment, reduce the continuity of the alloyed layer of the zinc coating.

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Authors and Affiliations

D. Kopyciński
E. Guzik
A. Szczęsny
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Abstract

It is assumed that close to the margins of ice-sheets, glacial, fluvial and aeolian processes overlap, and combined with weathering processes, produce numerous sediments, in which quartz is a common mineral. Quartz grains, if available, may serve as a powerful tool in determining the depositional history, transportation mode and postdepositional processes. However, quartz grain studies in some modern glacial areas are still sparse. In this study, we examine for the first time quartz grains sampled from the modern glacial and proglacial environments of the Russell Glacier, southwest Greenland in binocular microscope and scanning electron microscope, to analyze their shape, character of surface and microtextures. We debate whether the investigated quartz grains reveal glacial characteristics and to what extent they carry a signal of another transportation and sedimentary processes. Although glacial fracturing and abrasion occur in grain suites, most mechanical origin features are not of a high frequency or freshness, potentially suggesting a reduced shear stress in the glacier from its limited thickness and influence of the pressurized water at the ice-bed. In contrast, the signal that originates from the fluvial environment is much stronger derived by numerous aqueous-induced features present on quartz grain surfaces. Aeolian-induced microtextures on grain surfaces increase among the samples the closest to the ice margin, which may be due to enhanced aeolian activity, but are practically absent in sediments taken from the small scale aeolian landforms. In contrast, aeolian grains have been found in the bigger-size (1.0-2.0 mm) investigated fraction. These grains gained the strongest aeolian abrasion, possibly due to changes in transportation mode.
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Authors and Affiliations

Edyta KALIŃSKA-NARTIŠA
Kristaps Lamsters
Jānis Karušs
Māris KRIEVĀNS
Agnis REČS
Raimonds Meija
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Abstract

The efficient, stable and reliable operation of the blast furnace secures the proper quality of coke, which is one of the basic components of the blast furnace charge. In modern blast-furnace technology, when using substitute fuels, i.e. coal dust, the role of coke is extremely important. For this reason, the demands placed on its quality increase. Domestic coking plants have a limited base of Polish high quality coking coals at their disposal, therefore the full use of their coking properties is extremely important. The grain composition of the coal blend is one of the basic factors affecting the quality of the produced coke. This influence depends on the quantity and quality of coal components that make up the blend. In the conducted research, 21 coking coals, differing significantly in the degree of rank and origin (Polish and overseas coals), it was shown that the separated grain classes differ in properties, both coking properties and the degree of devolatalization during heating. In analyzing the obtained results, it was observed that the grain volume growth occurs essentially in the temperature range between the beginning and the maximum of fluidity. It has been shown that there is a linear correlation between the temperature corresponding to maximum fluidity and the temperature at which the maximum rate of evolution of volatiles enters. The presented phenomena accompany the emergence of coal expansion pressure during the coking process and they are its primary causes. The presented results can be an important guide for preparing the milling of coal for the coking process.

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Authors and Affiliations

Bartosz Mertas
Marek Ściążko
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Abstract

Wheat grain discoloration, a worldwide disease that lowers grain quality and decreases grain yield, does not have a single etiology. It has been proposed that it is a consequence of an abiotic mechanism, a response to environmental conditions or enzymatic activity. It has also been suggest that it is a biotic mechanism, a fungal infection principally by Alternaria spp. and Bipolaris sorokiniana. The present work was carried out to analyze the possible etiology of this disease in nine durum wheat genotypes from two localities of southern Buenos Aires province (Argentina) on two sowing dates. Incidence (percentage of grain discoloration) was recorded and mycobiota associated with this pathology was registered following ISTA rules. Peroxidase activity in an extract obtained from grains belonging to genotypes of the locality that showed the highest incidence was measured.

The incidence among genotypes, localities and sowing dates varied, although the genotypes with the higher and lower values of incidence were the same for all the variables tested. The fungus Alternaria spp. was isolated the most frequently followed by Fusarium spp., while Bipolaris sorokiniana was found the least frequently. Peroxidase activity showed that all the treatments had similar levels of enzymatic activity, but there was no clear differentiation between controls either between genotypes with the lowest or the highest incidence values. This suggests that peroxidase activity did not have a clear relationship with grain discoloration. In this research, it is presumed that fungal infection is the main cause of this disease.

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Authors and Affiliations

Maria Josefina Cipollone
Paulina Moya
Iván Martínez
Mario Saparrat
Marina Sisterna
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Abstract

The use of cold forging is a widely used solution in many industries. One application is the manufacture of bolts and fasteners. The largest amounts of bolts are used in the automotive and machine industry. Those customers demand high standards of quality and reliability from producers based on ISO 9001 and IATF 16949. Also, the construction, agriculture and furniture industries are raising their expectations for deliveries from year to year.
Automotive companies issue their standards specifying specific requirements for products. One of these standards is the aviation standard SAE USCAR 8-4; 2019, which speaks of a compatible arrangement of fibers in the bolt head and in the area of transition into the mandrel.
The article presents the cold forging process of flange bolts. Obtaining a compatible, acceptable and incompatible grain flow pattern based of the above mantioned standard was presented. Then the results of FEM simulation were correlated with the performed experiment.
The effect of incompatible grain flow system was discussed and presented as the crack initiating factor due to delta ferrite, hydrogen embrittlement, tempering embrittlement. The reliability of the connections was confirmed in the assembly test for yield stress on a Schatz machine. The advantages of this method and the difference compared to the tensile test were presented.
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Bibliography

[1] IA TF 16949: 2016 – Automotive Quality Management System Standard.
[2] ISO 9001: 2015 – Systemy zarządzania jakością – Wymagania.
[3] A. Komornicka, M. Sąsiadek, T. Nahirny, Wyzwania przemysłu motoryzacyjnego w świetle wprowadzania standardów IATF 16949:2016, [in:] R. Knosali, Innowacje w Zarządzaniu i Inżynierii Produkcji, Oficyna Wydawnicza Polskiego Towarzystwa Zarządzania Produkcją.
[4] S. Ziółkiewicz, S. Stachowiak, D. Kaczmarczyk, A. Karpiuk, Obróbka Plastyczna Metali 17 (1), 7-13 (2006).
[5] A. Żmudzki, P. Skubisz, J. Sińczak, M. Pietrzyk, Obróbka Plastyczna Metali 17 (3), 9-19 (2006).
[6] N . Biba, S. Stebounov, A. Lishiny, J. Mater. Process. Tech. 113, 34-39 (2001).
[7] M Saad, S. Akhtar, M. Srivastava, J. Chaurasia, Materials Today: Proceedings 5, 19576-19585 (2018).
[8] A . Dubois, L. Lazzarotto, L. Dubar., J. Oudin, Wear 249, 951-961 (2002).
[9] Y . Nugraha, Theory of WireDrawing, Tirtayasa University (2007).
[10] S.Y. Hsia, Y.T. Chou, J.C. Chao, Advances in Mechanical Engineering 8 (3), 1-10 (2016).
[11] R . Bussoloti, L. Albano, L. de Canale, G.E. Totten, Delta Ferrite: Cracking of Steel Fasteners, [in:] R. Colás, G.E. Totten, Encyclopedia of Iron, Steel, and Their Alloys, Five-Volume Set, CRC Press (2006).
[12] D .H. Herring, Indust Heat 73 (16), 9 (2006).
[13] S.V. Brahimi, S. Yue, K.R. Sriraman, Philos. Trans. A Math. Phys. Eng. Sci. 375 (2098), (2017).
[14] SAE USCAR 8-4;2019 „Grain Flow Pattern for Bolts, Screws and Studs”.
[15] PN -EN 26157-3. Części złączne – Nieciągłości powierzchni – Śruby, wkręty i śruby dwustronne specjalnego stosowania.
[16] ISO 898-1:2013-06 Własności mechaniczne części złącznych wykonanych ze stali węglowej oraz stopowej – Część 1: Śruby i śruby dwustronne o określonych klasach własności – Gwint zwykły i drobnozwojny.
[17] ISO 16047:2007 Części złączne – Badanie zależności moment obrotowy/siła zacisku.
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Authors and Affiliations

T. Dubiel
1
ORCID: ORCID
T. Balawender
2
ORCID: ORCID
M. Osetek
1
ORCID: ORCID

  1. Koelner Rawlplug IP Sp. z o. o. Oddział w Łańcucie / Rzeszów University of Technology, Poland
  2. Rzeszów University of Technology, 12 Powstańców Warszawy Av., 35-959 Rzeszów, Poland
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Abstract

In this work, 25 wheels were cast with three different grain refiners: Al5Ti1B, Al3Nb1B and MTS 1582. Samples were machined from the wheels to check the mechanical properties. It was found that Nb grain refinement had the lowest grain size (260 mm) and highest tensile properties (yield strength of 119-124 MPa and ultimate tensile strength of 190-209 MPa). Al5Ti1B and MTS 1582 revealed quite similar results (110 MPa yield and 198 MPa ultimate tensile strength). The fading of the grain refining effect of Al5TiB1 master alloy was observed in both Nb and Ti added castings whereas during the investigated time interval, the fading was not observed when MTS 1582 was used.
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Authors and Affiliations

F. Aydogan
1
K.C. Dizdar
2
ORCID: ORCID
H. Sahin
2
ORCID: ORCID
E. Mentese
1
D. Dispinar
2
ORCID: ORCID

  1. Doktas Wheels, Turkey
  2. Istanbul Technical University, Turkey
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Abstract

A fading mechanism during casting of treated Al-B-Sr master alloys in an aluminium-silicon cast alloy was investigated. Two different master alloys, the Al-3%B-3%Sr and Al-4%B-1%Sr were demonstrated for the efficiency test both grain refinement and modification microstructure. From experimental result, the addition of Al-3%B-3%Sr master alloy led to a refined grain size and fully modified eutectic Si. However, smaller grain sizes were found with Al-4%B-1%Sr master alloy addition while eutectic Si had coarser acicular morphology. The formation of high amounts of SrB6 compound in the Al-3%B-3%Sr master alloy resulted to increase of grain size and eutectic Si. In fading mechanism test when holding the melt for prolong time, the agglomeration of the SrB6 and AlSiSr compounds at the bottom of the casting specimen was important factors that decreased both grain refinement and modification efficiency. The stirring of the melt before pouring was found that the grain size and Si morphology were improved.
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Authors and Affiliations

P. Muangnoy
1
ORCID: ORCID
K. Eidhed
1
ORCID: ORCID

  1. University of Technology North Bangkok, Faculty of Engineering, Department of Materials and Production Technology Engineering, King Mongkut’s Bangkok, Thailand
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Abstract

A desirable property of iterated cryptographic algorithms, such as stream ciphers or pseudo-random generators, is the lack of short cycles. Many of the previously mentioned algorithms are based on the use of linear feedback shift registers (LFSR) and nonlinear feedback shift registers (NLFSR) and their combination. It is currently known how to construct LFSR to generate a bit sequence with a maximum period, but there is no such knowledge in the case of NLFSR. The latter would be useful in cryptography application (to have a few taps and relatively low algebraic degree). In this article, we propose a simple method based on the generation of algebraic equations to describe iterated cryptographic algorithms and find their solutions using an SAT solver to exclude short cycles in algorithms such as stream ciphers or nonlinear feedback shift register (NLFSR). Thanks to the use of AIG graphs, it is also possible to fully automate our algorithm, and the results of its operation are comparable to the results obtained by manual generation of equations. We present also the results of experiments in which we successfully found short cycles in the NLFSRs used in Grain-80, Grain-128 and Grain-128a stream ciphers and also in stream ciphers Bivium and Trivium (without constants used in the initialization step).

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Authors and Affiliations

Władysław Dudzic
Krzysztof Kanciak
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Abstract

The results of researches of sorption processes of surface layers of components of sand moulds covered by protective coatings are

presented in the hereby paper. Investigations comprised various types of sand grains of moulding sands with furan resin: silica sand,

reclaimed sand and calcined in temperature of 700oC silica sand. Two kinds of alcoholic protective coatings were used – zirconium and

zirconium – graphite. Tests were performed under condition of a constant temperature within the range 30 – 35oC and high relative air

humidity 75 - 80%. To analyze the role of sand grains in sorption processes quantitavie moisture sorption with use of gravimetric method

and ultrasonic method were used in measurements. The tendency to moisture sorption of surface layers of sand moulds according to the

different kinds of sand grains was specified. The effectiveness of protective action of coatings from moisture sorption was analyzed as

well.

Knowledge of the role of sand grains from the viewpoint of capacity for moisture sorption is important due to the surface casting defects

occurrence. In particular, that are defects of a gaseous origin caused by too high moisture content of moulds, especially in surface layers.

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Authors and Affiliations

N. Kaźnica
J. Zych
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Abstract

The modification is a widespread method of improving the strength properties of cast iron. The impact in terms of increasing amounts of

eutectic grains has been thoroughly studied while the issue of the impact on the mechanical properties of primary austenite grains has not

been studied in depth yet. The paper presents the study of both aspects. The methodology was to conduct the melting cast iron with flake

graphite, then modifying the alloy by two sets of modifiers: the commercial modifier, and a mixture of iron powder with a commercial

inoculant. The DAAS test was carried out to identify the primary austenite grains. The degree of supercooling was determined and the

UTS test was performed as well. Additionally carried out the metallographic specimen allowing for counting grains. It can be concluded

that the introduction of the iron powder significantly improved the number of austenite primary grains which resulted in an increase

in tensile strength UTS.

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Authors and Affiliations

D. Kopyciński
E. Guzik
A. Szczęsny
J. Dorula
D. Siekaniec
M. Ronduda
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Abstract

The aim of this paper was to attain defect free, pure copper castings with the highest possible electrical conductivity. In this connection, the effect of magnesium additives on the structure, the degree of undercooling (ΔTα = Tα-Tmin, where Tα – the equilibrium solidification temperature, Tmin – the minimum temperature at the beginning of solidification), electrical conductivity, and the oxygen concentration of pure copper castings have been studied. The two magnesium doses have been investigated; namely 0.1 wt.% and 0.2 wt.%. A thermal analysis was performed (using a type-S thermocouple) to determine the cooling curves. The degree of undercooling and recalescence were determined from the cooling and solidification curves, whereas the macrostructure characteristics were conducted based on a metallographic examination. It has been shown that the reaction of Mg causes solidification to transform from exogenous to endogenous. Finally, the results of electrical conductivity have been shown as well as the oxygen concentration for the used Mg additives.

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Authors and Affiliations

M. Kranc
A. Garbacz-Klempka
M. Górny
G. Sikora
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Abstract

The paper presents the results of basic research on the influence of the properties of sand grains on electrical properties of water glass

moulding sands. It shows electrical properties of the main component – sand grains, crucial to the kinetics of moulding sands heating, such

as permittivity εr and loss factor tgδ. Measurements were carried out with the use of the perturbation method for silica, chromite and

olivine sands of different mineral, chemical composition and particle size distribution, as well as for moulding sands with water glass

grade 145. Analysis of the results of measurements of electrical properties shows that all moulding sands are characterized by a similar

permittivity εr and loss factor tgδ. It was found that the electrical properties and the quantity and quality of other components may have

a decisive influence on the effectiveness and efficiency of the microwave heating of moulding sands with sand grains. In determining the

ability to efficiently absorb the microwave radiation for mixtures which moulding sands are, the impact of all components influencing their

individual technological parameters should be taken into account.

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Authors and Affiliations

B. Opyd
K. Granat
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Abstract

The present research was conducted on thin-walled castings with 5 mm wall thicknesses. This study addresses the effect of the influence of

different master alloys, namely: (1) Al-5%Ti-1%B, (2) Al-5%Ti and (3) Al-3%B, respectively on the structure and the degree of

undercooling (ΔTα = Tα-Tmin, where Tα - the equilibrium solidification temperature, Tmin - the minimum temperature at the beginning of

α(Al) solidification) of an Al-Cu alloy. The process of fading has been investigated at different times spent on the refinement treatment ie.

from 3, 20, 45 and 90 minutes respectively, from the dissolution of master alloys. A thermal analysis was performed (using a type-S

thermocouple) to determine cooling curves. The degree of undercooling and recalescence were determined from cooling and solidification

curves, whereas macrostructure characteristics were conducted based on a metallographic examination. The fading effect of the refinement

of the primary structure is accompanied by a significant change in the number (dimension) of primary grains, which is strongly correlated

to solidification parameters, determined by thermal analysis. In addition to that, the analysis of grain refinement stability has been shown

with relation to different grain refinements and initial titanium concentration in Al-Cu base alloy. Finally, it has been shown that the

refinement process of the primary structure is unstable and requires strict metallurgical control.

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Authors and Affiliations

M. Górny
M. Kawalec
G. Sikora
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Abstract

The samples of the CuCr0.6 alloy in the solution treated and additionally in aging states were severely plastically deformed by compression with oscillatory torsion (COT) method to produce ultrafine – grained structure. The samples were processed by using process parameters as: frequency of torsion (f = 1.6 Hz), compression speed (v = 0.04 mm/s), angle torsion (α = ±6°), height reduction (Δh = 7 mm). The total effective strain was εft = 40. The microstructure has been analyzed by scanning transmission electron microscope (STEM) Hitachi HD-2300A equipped with a cold field emission gun at an accelerating voltage of 200 kV. The quantitative microstructure investigations as disorientation angles were performed using a FEI INSPECT F scanning electron microscope (SEM) equipped with a cold field emission gun and a electron backscattering diffraction (EBSD) detector. The mechanical properties were determined using MST QTest/10 machine equipped with digital image correlation (DIC). The COT processed alloy previously aged at 500°C per 2h shows high mechanical strength, ultimate tensile strength UTS: 521 MPa and yield tensile strength YS: 488 MP attributed to the high density of coherent precipitates and ultrafine grained structure.

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Authors and Affiliations

A. Urbańczyk-Gucwa
A. Brzezińska
K. Rodak
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Abstract

The embryology of three polar flowering plants of the family Caryophyllaceae was studied using the methods and techniques of the light, normal and fluorescence microscopes, and the electron microscopes, scanning and transmission. The analyzed species were Colobanthus quitensis of West Antarctic (King George Island, South Shetlands Islands) as well as Cerastium alpinum and Silene involucrata of the Arctic (Spitsbergen, Svalbard). In all evaluated species, flowering responses were adapted to the short Arctic and Australian summer, and adaptations to autogamy and anemogamy were also observed. The microsporangia of the analyzed plants produced small numbers of microspore mother cells that were differentiated into a dozen or dozens of trinucleate pollen grains. The majority of mature pollen grains remained inside microsporangia and germinated in the thecae. The monosporous Polygonum type (the most common type in angiosperms) of embryo sac development was observed in the studied species. The egg apparatus had an egg cell and two synergids with typical polarization. A well-developed filiform apparatus was differentiated in the micropylar end of the synergids. In mature diaspores of the analyzed plants of the family Caryophyllaceae, a large and peripherally located embryo was, in most part, adjacent to perisperm cells filled with reserve substances, whereas the radicle was surrounded by micropylar endosperm composed of a single layer of cells with thick, intensely stained cytoplasm, organelles and reserve substances. The testae of the analyzed plants were characterized by species-specific primary and secondary sculpture, and they contained large amounts of osmophilic material with varied density. Seeds of C. quitensis, C. alpinum and S. involucrata are very small, light and compact shaped.
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Authors and Affiliations

Wioleta Kellmann-Sopyła
Irena Giełwanowska
Justyna Koc
Ryszard J. Górecki
Marcin Domaciuk
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Abstract

Eighteen sediment samples from a 36 cm long sediment core retrieved from a proglacial lake (namely P 11) situated in the Schirmacher Oasis, East Antarctica, were analysed for the study of quartz grain morphology and microtexture, along with sand percentage, to reconstruct the paleoenvironmental changes in the lake during the Holocene. The age of the core ranges from 3.3 ka BP to 13.9 ka BP. The quartz grain morphology and microtexture reveal significant evidences of glacial transport along with some eolian and aqueous activities. On the basis of predominance of these signatures and the zonation from CONISS Cluster Analysis on the percentages of characteristic grain morphology and microtextures, the entire core has been subdivided into three major zones. From the paleoenvironmental perspective, it can be concluded that there is an onset of interglacial period at the advent of Holocene (12.3 ka BP), which reigned until 5.3 ka BP and thereafter, again a glacial environment prevailed until 3.3 ka BP with some variations in-between. The results indicate probable alternative colder and less colder phases in the study area, which are also well supported by the respective sand percentages in the sediments. © 2017 Polish Academy of Sciences 2017.
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Authors and Affiliations

Abhijit Mazumder
Pawan GOVIL
Ratan Kar
Narath Meethal Gayathri
RAGHURAM
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Abstract

The paper presents results of aluminium concentration determination in the samples of surface water and bottom sediments of the Mala Wełna River (West Poland). In the surface water the concentration of aluminium varies in the range from 4.14 to 25.9 ug/dm'. With use of the Mineql+ program the concentration of the aluminium sulphate complexes in the water samples studied has been determined in a model way. In the bottom sediments samples of the river aluminium has been determined in the granulometrie fractions of the grain sizes> 2.0; 2.0-1.0; 1.0-0.5; 0.5-0.25; 0.25-0.1; 0.1-0.063; < 0.063 mm, using the sequential extraction scheme proposed by Tessier el al. The lowest concentration of aluminium has been found in the granulometrie fraction 0.5-0.25 mm, while the highest in the fractions 0.1-0.063 and< 0.063 mm. An elevated concentration of aluminium has been also noted in the fraction> 2.0 mm. Taking into regard the chemical fractions the lowest concentration of aluminium has been found in the exchange fraction and the fraction bounded to carbonates (fractions I and li), whereas the highest concentration of aluminium has been determined in the lithogenic fraction (fraction V). The methods of sample preparation for analysis of aluminium in bottom sediments were compared. Il was observed that higher concentration of aluminium was present in grounded samples without its influence on grain size fractions. The concentration of aluminium in surface water samples has been determined by the GF-AAS, while in bottom sediments by F-AAS.
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Authors and Affiliations

Marcin Frankowski
Anetta Zioła-Frankowska
Jerzy Siepak
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Abstract

Straw, particularly cereal straw, is a valuable by-product of crop production, which can be used for various purposes, e.g. as livestock feed and bedding or for making fuels, however it should primarily be retained on farmland in order to prevent soil organic matter (SOM) losses and thus to maintain or improve soil quality. The aim of this study was to analyze effects of the frequency of crop residues (straw) incorporation into the soil on the content of soil organic matter and on crop yields. There were the following experimental treatments: SR – straw of all crop in the rotation removed, S1 – straw of one crop per rotation incorporated, S2 – straw of two crops in the rotation incorporated, and S3 – straw of three crops incorporated into the soil (loamy sand). After 21 years of crop rotation with straw removal (SR) the SOM level in the soil slightly decreased to 14.4 g∙kg –1 soil DM, compared to that in 1997 (14.6 g∙kg –1). However, when straw of one crop (rape) per rotation was incorporated (S1) the content of SOM increased to 15.0 g∙kg -1 soil DM, and to 15.6 and 16.0 g∙kg –1 in S2 and S3 treatments respectively. Straw retention had also a beneficial effect on the content of labile fractions of SOM (hot water extractable C and N). Grain yields and yield components of wheat and triticale, and seed yields of rape in the SR treatment were not significantly different from those obtained in S1, S2 and S3 treatments.
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Authors and Affiliations

Janusz Smagacz
1
ORCID: ORCID
Stefan Martyniuk
1
ORCID: ORCID

  1. Institute of Soil Science and Plant Cultivation – State Research Institute, Czartoryskich 8, 24-100 Puławy, Poland
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Abstract

The research was conducted in Tartous Governorate during the two agricultural seasons (2018–2019 and 2019–2020) under control conditions, the aim of the research is to study the relationship between the productivity of five promising strains of bread wheat (‘ACSAD 1256’, ‘Douma 58847’, ‘Douma 58585’, ‘Douma 64453’, ‘ACSAD 1149’) and two cultivars (‘Douma 2’ and ‘Douma 4’) and some quantitative indicators of drought: stress tolerance index ( STI), mean of productivity ( MP), modified stress tolerance index ( MSTI), and relative yield ( RY).
Cultivation was carried out in pots filled with light sandy silty soil, and three treatments of 70, 50, and 30% of the field capacity were applied in addition to the control and with three replications for each treatment.
The strains ‘Douma 58585’ and ‘Douma 58847’ gave high yield values for grain in the two agricultural seasons. It was also found that there were significant differences between the two seasons in yield between the control and drought stress factors and drought tolerance indicators, such as stress tolerance index, modified stress tolerance index ( MSTI), mean of productivity ( MP), and relative yield ( RY).
On the other hand, a positive and strong relationship was found between STI, MSTI, and MP in both treatments and both seasons. The research concluded that the best indicators, which were related to the productivity, whether in the control or transactions and in the two growing seasons together, are STI and MP, which are promising indicators in the classification of stress-tolerant cultivars or strains.
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Authors and Affiliations

Lubna Barhom
1
Hayat Touchan
2
ORCID: ORCID

  1. Tishreen University, Faculty of Agriculture, Field Crops Department, Lattakia, Syria
  2. Aleppo University, Faculty of Agriculture, Field Crops Department, 12212, Aleppo, Halab, Syria

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