The influence of the hold time of the austempering heat treatment at 280°C on the microstructure and corrosion resistance in NaCl-based media of austempered ductile iron was investigated using X-ray diffraction, micro-hardness measurements, corrosion tests and surface observations. Martensite was only found in the sample which was heat treated for a short period (10 minutes). Corrosion tests revealed that this phase does not play any role in the anodic processes. Numerous small pits were observed in the α-phase which is the precursor sites in all samples (whatever the value of the hold time of the austempering heat treatment).
The research article address, the mechanical properties such as fatigue, impact strength and tribological properties of Austempered ductile iron (ADI) has been investigated. The samples of ADI iron were austenitized at 927°C for 2 hrs and later it was under austempering process for 2 hrs at a temperature range of 240°C to 400°C. Experiments under axial loading has been carried out on three different compositions (without Ni(X), 0.22 wt % Ni (X1), 0.34 wt. % Ni (X2). Fabricated test bars were converted in to as per ASTM standard samples for different tests. In order to study the influence of chunky nickel morphology studies on fatigue life and impact strength were carried out on a second set of specimens without any microstructural defect. Metallurgical analyses were performed on all the samples of heat treated samples (AF – Ausferrite, MB – Mixed bainite, M – Martensite, RA – Retained Austenite and N-Nodule) were found and compared. It was found that a mean content of 22% of chunky nickel in the microstructure (with respect to total Ni content) influence considerably the fatigue and impact strength properties of the cast iron. Moreover tribological properties of the specimens were also studied under dry sliding conditions at various sliding speed and load. The wear resistance and coefficient of friction were found to increase with increase in load and sliding speed.
This work deals with the effect of austempering temperature and time on the microstructure and content of retained austenite of a selected cast steel assigned as a material used for frogs in railway crossovers. Bainitic cast steel was austempered at 400°C, 450°C and 500°C for two selected times (0.5 h, 4.0 h) to study the evolution of the microstructure and retained austenite content. The microstructure was characterized by optical microscopy, X-ray diffraction analyses (XRD), and hardness tests. Phase transformations during and after austempering were determined by dilatometric methods.
The increase in isothermal temperature causes an increase in time to start of bainitic transformation from 0.25 to 1.5 s. However, another increase in temperature to 500°C shifts the incubation time to as much as 11 s. The time after which the transformations have ended at individual temperatures is similar and equal to about 300 s (6 min.). The dilatation effects are directly related to the amount of bainite formation. Based on these we can conclude that the temperature effect in the case of cast steel is inversely proportional to the amount of bainite formed. The largest effect can be distinguished in the case of the sample austempered at 400°C and the smallest at 500°C. Summarizing the dilatometric results, we can conclude that an increase in austempering temperature causes an increase in austenite stability. In other words, the chemical composition lowers (shifts to lower temperatures) the range of bainite transformation. It is possible that at higher austempering temperatures we will receive only stable austenite without any transformation. This is indicated by the hatched area in Figure 4b. This means that the heat treatment of cast steel into bainite is limited on both sides by martensitic transformation and the range of stable austenite. The paper attempts to estimate the content of retained austenite with X-ray diffraction.
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