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Abstract

The Fe-based alloy with manganese led to the appearance of new austenitic alloys, with the antiferromagnetic property pursued, resulting in compatibility with the magnetic field as that of magnetic resonance imaging. The corrosion resistance behavior of the biodegradable Fe-Mn-Si alloy was analyzed in a thermostatic chamber at 37±1°C for 24, 48 and 72 hours by immersing in Ringer solution. Also, the cast and laminated samples were subjected to electro-corrosion tests using a potentiostat equipment. Linear and cyclic potentiometry is presented for characterize the corrosion behavior of the experimental samples in electrolyte. Due to the interaction between the alloy and the liquid medium a change in the solution pH was observed. Structure analysis and chemical composition details of the surfaces were obtained using electron scanning microscopy (SEM) and X-ray energy dispersive spectroscopy (EDS).
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Authors and Affiliations

A.-M. Roman
1
ORCID: ORCID
R. Chelariu
1
ORCID: ORCID
R. Cimpoesu
1
ORCID: ORCID
I. Stirbu
1
ORCID: ORCID
I. Ionita
1
ORCID: ORCID
M.M. Cazacu
2
ORCID: ORCID
B.A. Prisecariu
3
ORCID: ORCID
N. Cimpoesu
3
ORCID: ORCID
P. Pietrusiewicz
4
ORCID: ORCID
A. Sodor
3
ORCID: ORCID

  1. Faculty of Materials Science and Engineering, “Gheorghe Asachi” Technical University of Iasi, Prof.dr.doc. D. Mangeron no. 41 Street, 700050 Iasi, Romania
  2. “Gheorghe Asachi” Technical University of Iasi, Department of Physics, 700050 Iasi, Romania
  3. “Grigore T. Popa” University of Medicine and Pharmacy of Iasi, 16 Univ. Street, 700115 Iasi, Romania
  4. Częstochowa University of Technology, Department of Physics , 42-200 Częstochowa, Poland
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Abstract

The effect of TiC content on the microstructure and mechanical properties of a nanocrystalline Fe-Mn alloy was investigated by XRD analysis, TEM observation, and mechanical tests. A sintered Fe-Mn alloy sample with nano-sized crystallites was obtained using spark plasma sintering. Crystallite size, which is used as a hardening mechanism, was measured by X-ray diffraction peak analysis. It was observed that the addition of TiC influenced the average size of crystallites, resulting in a change in austenite stability. Thus, the volume fraction of austenite at room temperature after the sintering process was also modified by the TiC addition. The martensite transformation during cooling was suppressed by adding TiC, which lowered the martensite start temperature. The plastic behavior and the strain-induced martensite kinetics formed during plastic deformation are discussed with compressive stress-strain curves and numerical analysis for the transformation kinetics.

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Authors and Affiliations

Junhyub Jeon
ORCID: ORCID
Seunggyu Choi
Namhyuk Seo
ORCID: ORCID
Young Hoon Moon
In-Jin Shon
Seok-Jae Lee
ORCID: ORCID

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