Applied sciences

Archives of Metallurgy and Materials

Content

Archives of Metallurgy and Materials | 2025 | vol. 70 | No 4

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Abstract

The study analyzed two selected representative HSLA steels rolled at the Krakow branch of ArcelorMittal Poland S.A. The aim of the analysis was to determine the effect of parameters such as strain and cooling rate on the onset temperature of the transformation from austenite to ferrite. Dilatometric tests were carried out, followed by strain dilatometry. The cooling rate was varied and its relationship with the temperature of the beginning of austenite to ferrite transformation (Ar3) was determined. In the second part of the study, the subject literature was analyzed to find out how quickly the Ar3 temperature could be calculated. The available equations for calculating the Ar3 temperature were checked. However, the results of the calculations were not consistent enough to use these equations in the actual process. Therefore, the authors decided to develop their own equation – the proposed solution allows the calculation of the Ar3 temperature for the two selected HSLA steels mentioned above with an accuracy of several degrees and a correlation of more than 90%.
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Authors and Affiliations

Tomasz Hamryszczak
1
ORCID: ORCID
M. Zapf
T. Śleboda
ORCID: ORCID
G. Korpała
U. Prahl
ORCID: ORCID

  1. AGH University of Krakow, Poland; ArcelorMittal Poland S.A., Krakow, Poland
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Abstract

To resolve coating appearance non-uniformity in industrial PVD-coated cutting tools, this study investigates cathode system gas distribution optimization. By analyzing the gas flow characteristics of single-nozzle-type gas pipelines, finite element simulations were employed to compare gas flow fields under equal hole spacing and gradient hole spacing configurations. Structural optimizations, including downward nozzle orientation and diffusion space enlargement, were proposed to eliminate jet flow effects. Experimental results demonstrated that the gradient hole spacing design significantly improved coating uniformity. Energy-dispersive spectroscopy (EDS) analysis revealed that the carbon content deviation among upper, middle, and lower samples was less than 10%, effectively resolving axial chromatic inconsistencies. This work establishes theoretical frameworks and technical protocols for PVD gas distribution uniformity, advancing product quality and batch consistency.
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Authors and Affiliations

Zhao Jiang
1
Zhanji Ma
1
Shuilian Luo
1
Yanshuai Zhang
1

  1. National Key Laboratory on Vacuum Technology and Physics, Lanzhou Institute of Physics, Lanzhou 730000, P.R. China
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Abstract

This study aimed to design and prepare FeCoNi (AlSi)0.2,0.4,0.6 high-entropy alloy (HEA) magnetic powder and bulk by MA and spark plasma sintering (SPS), and to investigate the effects of AlSi variations on the microstructure evolution and magnetic properties of HEAs. A decrease in AlSi content promoted the precipitation of stratification faults (SFs) and twins from the face-centered cubic matrix. The addition of AlSi nonmagnetic elements and the formation of SFs and twins had obvious effects on the magnetic properties of the HEA. FeCoNi(AlSi)0.4 had excellent magnetic properties with 140.26±0.05 emu/g magnetic saturation (Ms) and 1.35±0.02 Oe coercivity field (Hc), and the excellent magnetic properties are due to the thinning effect of the single atomic layer twin boundary on the magnetic domain and the short-range magnetic domain bonding effect between the magnetic domains. The results of this study will expand the design and application of high-entropy alloys in the field of high-performance magnetic materials.
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Authors and Affiliations

Xiaohua Li
1
ORCID: ORCID
Wenbing Li
1
ORCID: ORCID
Rui Wang
1
ORCID: ORCID
Enshun Ping
2
ORCID: ORCID
Shaofeng Yang
1
ORCID: ORCID

  1. Tianjin Key Laboratory of High Performance Precision Forming Technology and Equipment, Tianjin 300222, China
  2. Downhole Technology Service Company, CNPC Bohai Drilling Engineering Company Limited, Tianjin 300280, China
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Abstract

Due to the unique physicochemical properties of copper (Cu), conventional fusion welding faces certain challenges when welding this material. In this study, Cu-Cu joints were fabricated using refill friction stir spot welding (RFSSW) at five different plunge depths. The macroscopic morphologies of the welded joints (WJs) under various welding conditions were examined, and the microstructural differences in representative zones of the WJ were analyzed. The microhardness and tensile-shear failure load (T-SFL) of the WJs were evaluated to assess the mechanical performance, and the failure mechanisms were explored. The results indicated that with increasing plunge depth, the microstructure tended to coarsen, accompanied by a gradual decrease in microhardness. The T-SFL initially increased and then decreased with increasing plunge depth, with the optimal depth found to be 1.4 times the plate thickness. For Cu-Cu joints, the softening effect in the heat-affected zone (HAZ) outside the stirring zone is identified as a key factor limiting the load-bearing capacity of the WJs.
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Authors and Affiliations

Xiaole Ge
1 2
ORCID: ORCID
I.N. Kolupaev
1
ORCID: ORCID
Di Jiang
1 2
ORCID: ORCID
Shouzhen Cao
2
ORCID: ORCID
Weiwei Song
2
ORCID: ORCID
Hongfeng Wang
2
ORCID: ORCID

  1. National Technical University «Kharkiv Polytechnic Institute», Department of Materials Science, Kharkiv, 61002, Ukraine
  2. Huangshan University, College of Mechanical and Electrical Engineering, Huangshan, 245041, P.R. China
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Abstract

Heavy-duty vehicle gears play a vital role in transmission systems, but the harsh operating conditions they endure often lead to surface wear and deformation. To mitigate these effects, gears must possess optimal hardness and wear resistance. The use of surface coatings has proven to be an effective strategy for enhancing gear performance. In this study, a Cr2O3-reinforced coating was applied to gear surfaces using supersonic flame spraying technology. Microstructural, elemental, and phase analyses were carried out using X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy-dispersive spectroscopy (EDS) to evaluate the coating’s properties. The results revealed significant improvements in hardness, adhesion, and wear resistance, with the coated gear exhibiting a more compact surface microstructure. To further assess performance, solid models of both coated and uncoated gears were developed using ANSYS software. Static and fatigue life analyses indicated that the coated gear experienced reduced deformation and a longer service life. This study highlights the effectiveness of Cr2O3-reinforced coatings in the durability and overall performance of heavy-duty automotive gears.
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Authors and Affiliations

Ziyi Tan
1
ORCID: ORCID
Saihong Tang
1
ORCID: ORCID
B.T. Hang Tuah Baharudin
1
ORCID: ORCID
Rongbin Ma
2
ORCID: ORCID

  1. Universiti Putra Malaysia, Faculty of Engineering, Serdang, Selangor, 43400, Malaysia
  2. Nahua Ningbo New Materials Technology Co., Ltd, Ningbo City, 31500, China
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Abstract

Foreign object damage (FOD) is one of the main limiting factors for the life of aero-engine blades. In order to summarize the impact law and predict the damage gap caused by the impact of foreign objects on titanium alloy blades, the dynamic simulation calculation of foreign object damage at the inlet edge of an aero-engine guide vane was carried out with a specific blade as the research object, a cylindrical steel nail with high probability on the airport pavement as the foreign body and the most possible angle caused by the inlet flow field as the impact angle. The study found that: (i) The notch depth consists of two components: the initial depth at impact and the subsequent expansion due to centrifugal stress. (ii) The depth of the notch is always greater than the width. The maximum width of the notch is approximately equal to the cross-sectional diameter of the steel column. (iii) The relationship between notch depth and notch width is a quadratic function. (iv) The changes of notch depth with relative kinetic energy and steel column mass, and the changes of impact angle, maximum impact force and impact time with steel column mass are all power functions. With the increase of impact position, the relative kinetic energy of the steel column increases, and the change law is a quadratic function. (v) For the same foreign object, there is a critical value when the impact height increases. When the impact position is lower than it, the notch depth increases continuously. On the contrary, the notch depth decreases. Similarly, there is a critical value in the process of increasing relative kinetic energy. Smaller than it, the notch depth continues to increase, while larger than it, the notch depth continues to decrease. These findings provide data to support the diagnosis of blade damage under field conditions, and provide a theoretical basis for the design of blades against foreign object damage.
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Authors and Affiliations

Chunwang Li
1

  1. Xi’an International University, Engineering College, Xi’an, China
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Abstract

The main purpose of this research is the impact of graphene nanoparticle reinforcement on ballistic protection of composites and to investigate the ballistic and mechanical properties of these products. In this context nanocomposite ballistic plates were obtained by reinforcing different amounts of graphene to aramid-based composite plates after some processes. To characterize the graphene, several analyses were performed. Characteristic peaks were obtained by performing FTIR (Fourier Transform InFrared). Scanning Electron Microscopy (SEM) and Raman analyzes on graphene nanoplatelets used in the experimental study. Ballistic plates reinforced with graphene nanoplatelets and non-reinforced plates were subjected to shooting tests in the ballistic test laboratory in accordance with the NIJ (National Institute of Justice) standard and the test results were compared. As a result of the shooting tests, successful results were not achieved with ballistic plates reinforced with graphene and epoxy resin, except for one plate. This outcome was attributed to the negative impact of epoxy resin on the flexibility and energy absorption properties of the aramid layers. From a mechanical properties perspective, it was observed that the ultimate tensile strength of the samples with 0.5% and 1% by weight graphene increased.
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